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This book highlights major§achievements made in the last five years concerning sustainable C(sp 3 )-H§bond functionalization and offers a promising and emerging tool-kit for organic§synthesis. The book is divided into three chapters demonstrating key advances§in C(sp 3 )-H bond functionalization. Chapter 1 reviews§transition-metal-catalyzed C(sp 3 )-H bond functionalization using§different directing groups, while Chapter 2 addresses the new methods of§transition-metal-catalyzed and metal-free C(sp 3 )-H bond§functionalization without directing groups, in addition to briefly highlighting§redox-neutral C(sp 3 )-H bond functionalization. In closing, Chapter 3§examines visible-light photoredox catalysis, an emerging and highly sustainable§C(sp 3 )-H bond functionalization strategy. The book offers an§intriguing and useful reference guide for a broad readership working and/or§interested in the fields of organic, organometallic, and green chemistry.§§